Crystal structure of N/- (2-phenylacetyl) thiophene-2-carbohydrazide monohydrate
Crystal structure of N/- (2-phenylacetyl) thiophene-2-carbohydrazide monohydrate
C13H14N2O3S, monoclinic, C2/c (no. 15), a = 27.9910(12) Å, b = 6.5721(3) Å, c = 14.2821(7) Å, β = 92.600(3)°, V = 2624.6(2) Å3 , Z = 8, Rgt(F) = 0.042, wRref(F 2 ) = 0.105, T = 100 K. CCDC no.: 1479028 The crystal structure is shown in the gure. Tables 1 and 2 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters. Source of material Thiophene-2-carbonyl chloride (1.6 g, 11 mmol) in 10 mL dichloromethane was added dropwise to a mixture of
C13H14N2O3S, monoclinic, C2/c (no. 15), a = 27.9910(12) Å, b = 6.5721(3) Å, c = 14.2821(7) Å, β = 92.600(3)°, V = 2624.6(2) Å3 , Z = 8, Rgt(F) = 0.042, wRref(F 2 ) = 0.105, T = 100 K. CCDC no.:…
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