Practical Inorganic Chemistry 428Chem

 

 Chem. 428    2((0+2

Course Name: Practical Inorganic Chemistry
           Preparation of inorganic and organometallic complexes and using different techniques for separation and purification, applications in non-aqueous chemistry, spectroscopic studies and identification of the above complexes.
 Part one :Preparation Organometallic Compounds:
1- General idea about Technical FTIR  and Samples Preparation.
2- Preparation of Silver phenylacetylide Compound, [Ag(C2Ph)]n.
3- Preparation of Cobalt (III) Acetylacetonate, Co(acac)3.
4- { Preparation  [Tris(3-nitroacetylacetonato)] Cobalt(III)}.
Second part: Non-aqueous Titrations:
6- Determination of Molarity  Non-aqueous HClO4 acid.
7- Determination of Molarity  Non-aqueous HCl acid.
8- Determination of Molarity  Non-aqueous Ethanolamine.
Third Part: Specrophotometric Identification and Determination of complexes    
 9- Determination of the Composition of Complex:
a) The Slope Ratio Method.
b) The Continuous Variation Method.
10- Determination of the Equilibrium Constant by Hymann's Method.  
11- The Final Exam Theoretical and Practical.                                            
It should be note that, complete report about each experiment  must be handled with graph etc.